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Herein, we report on the synthesis of ferrocenylborole [Fc(BC4Ph4)2] featuring two borole moieties in the 1,1′‐positions. The results of NMR and UV/Vis spectroscopy and X‐ray diffraction studies provided conclusive evidence for the enhanced Lewis acidity of the boron centers resulting from the conjugation of two borole fragments. This finding was further validated by the reaction of [Fc(BC4Ph4)2]...
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