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The solvothermal reaction of the semirigid tritopic ligand 1,3,5‐tris[2,6‐dimethyl‐4‐(α‐carboxy)methoxyphenyl]benzene (H3BTA) with Zn(NO3)2 in a DEF/EtOH/H2O (4:2:1 v/v/v, DEF = N,N‐diethylformamide) mixture leads to the formation of three compositionally distinct coordination polymers (CPs) with different morphologies, that is, rods (Zn‐R), needles (Zn‐N), and blocks (Zn‐B), in the same pot at different...
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