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Old, limited data in the nuclear field is relied upon, but often requires revisiting for clarity. Like cracked glasses, flaws in old data can lead to missing information. Structural assumptions about PuIV oxalate hexahydrate have existed for decades, but only now has the structure been reported. These data have led to the identification of previously unreported coordination of water and changing oxalate...
Plutonium(IV) oxalate hexahydrate (Pu(C2O4)2 ⋅ 6 H2O; PuOx) is an important intermediate in the recovery of plutonium from used nuclear fuel. Its formation by precipitation is well studied, yet its crystal structure remains unknown. Instead, the crystal structure of PuOx is assumed to be isostructural with neptunium(IV) oxalate hexahydrate (Np(C2O4)2 ⋅ 6 H2O; NpOx) and uranium(IV) oxalate hexahydrate...
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