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We have successfully synthesised Ni75Fe25 nanostructured powders by means of low temperature (150 °C) hydrothermal method using sodium hydroxide (NaOH) as co-reduction agent. The powders are in fact large agglomerations of small nanoparticles with average diameters below 30 nm. The concentration of NaOH seems to play an important role in the final microstructure and morphology of the samples as deduced...
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