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A series of compounds Li_xMn_{3-x-y}Fe_yO_4 (x=1.0125;0≤y≤0.05) were synthesized by solid state reaction of Li_2CO_3 with the manganese oxide or iron-manganese oxide precursors. Investigations of the structure transformation effect of double substitution with Li^+ and Fe^{3+} ions in LiMn_2O_4, in the temperature range of 10-300 K, were undertaken using high-resolution X-ray powder diffraction at...
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