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The groundbreaking use of polyelectrolytes to increase the efficiency of supramolecular photocatalysts in solar H2 production schemes under aqueous aerobic conditions is reported. Supramolecular photocatalysts of the architecture [{(TL)2Ru(BL)}2RhX2]5+ (BL=bridging ligand, TL=terminal ligand, X=halide) demonstrate high efficiencies in deoxygenated organic solvents but do not function in air‐saturated...
Kleine Änderung mit großer Wirkung: Durch Überführen des endständigen Liganden in einen 4,7‐Diphenyl‐1,10‐phenanthrolin‐Rest wurden überlegene Ru,Rh,Ru‐Photokatalysatoren erhalten (siehe Schema; ocker Ru, rot Rh, blau N, gelb Cl oder Br), die photokatalytisch signifikant mehr H2 aus H2O erzeugen: H2O wird mit über 1300 Umsätzen pro Rh‐Zentrum und einer Maximaleffizienz von 7.3 % zu H2 reduziert.
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