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Biphenyl‐based arsine ligands were prepared in two‐step fashion by Pd‐catalyzed arsination and microwave‐assisted Suzuki–Miyaura coupling, providing sterically demanding arsine ligands in overall isolated yields up to 82 % as air‐stable solids. Short reaction times were achieved with the assistance of microwave irradiation in the direct and simple described protocol for the synthesis of biarylarsine...
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