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Herein, gelated thermoresponsive large‐compound vesicles (LCVs) are reported for the first time. The LCVs are prepared by self‐assembly of poly(ethylene oxide)‐block‐poly[N‐isopropylacrylamide‐random‐3‐(trimethoxysilyl)propyl methacrylate] [PEO‐b‐P(NIPAM‐r‐TMPM)] in DMF‐water mixture. Then, sol‐gel reaction of the reactive PTMPM block is performed to stabilize the LCVs. LCVs with higher cross‐linking...
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