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We report the space-selective precipitation of Cr3+-doped ZnAl2O4 crystals in aluminosilicate glass by femtosecond (fs) laser irradiation. The precipitation of ZnAl2O4 crystal was confirmed by x-ray diffraction (XRD), Raman spectra and transmission electron microscopy (TEM), and the incorporation of octahedron Cr3+ in ZnAl2O4 crystal was testified by electron paramagnetic resonance (EPR) and luminescence...
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