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Amorphous MoO3−x nanosheets were fabricated by the room‐temperature oxidation of molybdenum powder with H2O2, followed by light‐irradiation reduction in methanol. When applied as a substrate for surface‐enhanced Raman spectroscopy (SERS), these nanosheets exhibit higher sensitivity than the crystalline counterpart for a wide range of analytes. Moreover, the SERS activity remains stable on repeated...
The amorphous MoO3−x nanosheet exhibits more sensitive and stable surface‐enhanced Raman spectroscopy (SERS) activity than the crystalline counterpart. The signal is stable under repeated oxygen insertion/extraction condition, which allows the recycling of the substrate through H2O2‐based Fenton‐like reaction. More importantly, the interference‐free operando monitoring of the photocatalytic p‐nitrothiophenol...
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