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Single‐crystal X‐ray structure determinations of Ce4I6CN and disordered Ce6I9C2N phases are described together with electron‐microscopy studies of Ce6I9C2N and Y6I9C2N. Ce4I6CN crystallizes in the tetragonal space group P42/mnm with a = 13.877(2) Å, c = 9.665(2) Å. Compounds β′‐Ce6I9C2N and β″‐Ce6I9C2N crystallize in space group P6/m with a = 41.774(6) Å, c = 13.719(3) Å and a = 20.958(3) Å, c = 13...
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