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Four new ligands containing a pentasubstituted cyclopentadiene tethered to a stereogenic diamine unit have been prepared and used in the iron‐catalyzed enantioselective hydrosilylation of acetophenone. Catalytically active species have been generated in situ starting from various sources of iron. Fe(acac)2 was the catalyst precursor of choice, whereas other simple FeII or FeIII compounds resulted...
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