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The preparation and gas‐separation performance of self‐standing, high‐flux, graphene oxide (GO) membranes is reported. Defect‐free, 15–20 μm thick, mechanically stable, unsupported GO membranes exhibited outstanding gas‐separation performance towards H2/CO2 that far exceeded the corresponding 2008 Robeson upper bound. Remarkable separation efficiency of GO membranes for H2 and bulky C3 or C4 hydrocarbons...
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