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Carbonated chlorapatite nanopowders (n-CCAp) with different degrees of substitution were successfully synthesized by the one-step mechanochemical process. Results demonstrated that the formation of n-CCAp was influenced strongly by the carbonate content (x). From X-ray analysis, crystallite size, crystallinity degree, and unit cell volume of n-CCAp decreased significantly as carbonate content (x)...
Nanosized B-type carbonated fluorapatite (n-CFAp) with different degrees of substitution was successfully synthesized by a facile solid-state process. Results showed that a complex mechanochemical reaction occurred in several steps. Due to very high hydrophilic nature of P2O5, phosphoric acid was formed first, followed by the formation of anhydrous dicalcium phosphate and stoichiometrically carbonated...
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