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Oligomeric main‐chain Schiff‐base compounds 4 and 5 have been synthesized by the trans‐esterification of their respective doubly functionalized monomeric precursors [M{(η5‐C5H5)Fe(η5‐C5H4)C(=O)CH=C(4‐C6H4OH)NCH2CH2N=CH‐(2‐O,4‐CO2H–C6H3)}] [M = Ni (2), Cu (3)] in dmf. The new compounds were characterized by elemental analysis, FTIR and multidimensional NMR spectroscopy, mass spectrometry, and cyclic...
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