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What floats in the soup? Time‐course and ion‐mobility nano‐electrospray ionization (nESI) mass spectrometry probes the early aggregation states of an amyloidogenic endecapeptide derived from amino acid residues 105–115 of the human plasma protein transthyretin. A wide range of densely packed prefibrillar oligomers 1≤n≤13 are observed in dynamic populations over 8 h.
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