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A one‐pot method has been developed for the oxidative cleavage of internal alkenes into aldehydes by using 0.5 mol % of the nonheme iron complex [Fe(OTf)2(mix‐bpbp)] (bpbp=N,N′‐bis(2‐picolyl)‐2,2′‐bipyrrolidine) as catalyst and 1.5 equivalents of hydrogen peroxide and 1 equivalent of sodium periodate as oxidants. A mixture of diastereomers of the chiral bpbp ligand can be used, thereby omitting the...
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