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A facile route to synthesize amorphous TiO2 nanospheres by a controlled oxidation and hydrolysis process without any structure‐directing agents or templates is presented. The size of the amorphous TiO2 nanospheres can be easily turned from 20 to 1500 nm by adjusting either the Ti species or ethanol content in the reaction solution. The phase structure of nanospheres can be controlled by hydrothermal...
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