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The new tungsten iodide W15I47 was synthesized by reacting tungsten hexacarbonyl with iodine under elevated pressure and temperature conditions. The structure of W15I47 was refined by single‐crystal X‐ray diffraction with the non‐centrosymmetric space group C2 [Z = 2, a = 4088.3(4) pm, b = 952.3(1) pm, c = 1198.5(2) pm, and β = 103.97(1)°]. The characteristic motif in the structure is the square pyramidal...
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