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The selenium atom substitution for one of the capping chloride ligands in [Mo6(μ3-Cl8)Cl6]2– under the action of H2Se in situ results in a [Mo6(μ3-SeCl7)Cl6]3– cluster which is isolated and structurally characterized in the form of (Bu4N)3[Mo6(μ3-SeCl7)Cl6] (I). In the acetonitrile solution the complex exhibits luminescence (λmax = 775 nm, τem = 1.8 μs, Φem = 0.004). When the solution of I in acetonitrile...
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