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A chiral [M3L3]6+‐type nanobowl reported here was self‐assembled from cis‐protected mono‐palladium complex [(RRdiph)Pd](NO3)2 (where RRdiph= (1R,2R)‐(+)‐1,2‐diphenylethylenediamine) as chiral corners and 4,7‐phenanthroline ligand (L) as linkers in aqueous media. The hydrophobic cavity‐containing metallo‐macrocycle [Pd3L3]6+·6NO3 (1) with a syn, syn, syn orientation has been characterized by 1H NMR...
Seven dinuclear macrocyclic palladium(II) dithiocarbamates have been prepared from a homologous series of aliphatic 1,x‐diamines (x = 4–10); the objective was to vary systematically the size of the cavity. The resulting complexes were characterized by IR and NMR (1H, 13C) spectroscopy, high‐resolution FAB mass spectrometry, and in one case additionally by single‐crystal X‐ray diffraction analysis...
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