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Diastereoselective self‐assembly: Bis(pyridyl) ligands bearing a 2,8‐disubstituted Tröger's base scaffold undergo diastereoselective self‐assembly to yield discrete dinuclear achiral metallosupramolecular rhombs upon coordination to cis‐protected palladium(II) or platinum(II) ions in a self‐discriminating manner (see figure), whereas their analogues with a 3,9‐disubstituted Tröger's base core do not...
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