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The free‐radical oxidation reaction of cyclohexene is accomplished at 80°C in a 10:1 1,2‐dichloroethane:acetonitrile mixture under an air atmosphere using 0.05 molar equivalents of either tBuOOH or H2O2 and results in a 33.7% conversion yielding 23.7% 2‐cyclohexen‐1‐one, 8.0% 2‐cyclohexen‐1‐ol, and 2.0% cyclohexene oxide. With cyclooctene under similar conditions, a 42.3% conversion is obtained, 40...
New 3,3‐diphenylpropoxyphthalonitrile (5) was obtained from 3,3‐diphenylpropanol (3) and 4‐nitrophthalonitrile (4) with K2CO3 in DMF at 50 °C. The novel cobalt(II) phthalocyanine complexes, tetrakis‐[2‐(1,4‐dioxa‐8‐azaspiro[4.5]dec‐8‐yl)ethoxy] phthalocyaninato cobalt(II) (2) and tetrakis‐(3,3‐diphenylpropoxy)phthalocyaninato cobalt(II) (6) were prepared by the reaction of the phthalonitrile derivatives...
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