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Hydrated CaCl2, LiI, and MgCl2 salts induce self‐assembly in nonionic surfactants (such as C12H25(OCH2CH2)10OH) to form lyotropic liquid‐crystalline (LLC) mesophases that undergo a phase transition to a new type of soft mesocrystal (SMC) under ambient conditions. The SMC samples can be obtained by aging the LLC samples, which were prepared as thin films by spin‐coating, dip‐coating, or drop‐casting...
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