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The classical thermodynamics allow deriving theoretical expressions for the nucleation work and for the size of the critical nuclei in a supersaturated system. However, information on the rate of nucleus formation should be determined by means of kinetic considerations. This article sheds light on the nucleation kinetics in electrochemical systems at a constant thermodynamic supersaturation $$...
This report compares experimental data for the overpotential dependence of the stationary nucleation rate I st and of the induction time t o obtained in two different ways: (i) by varying the potential E n of the working electrode at a constant concentration of metal ions (standard pulse potentiostatic technique), and (ii) by varying the concentration of metal ions at...
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