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Starting from phthalic acid and Na[BH4], the low‐melting salt [EMIm+][BPB] [EMIm+ = 1‐ethyl‐3‐methylimidazolium; BPB– = bis(phthalato)borate] was synthesized and further reacted with Tb(NO3)3·6H2O to yield the one‐dimensional coordination polymer 1∞[Tb(o‐HBDC)(H2O)6][BPB]2. Product formation is a result of the formation of the ortho‐phthalato mono acid (o‐HBDC) from [BPB]– anions in the process and...
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