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The novel zinc borate Zn2B10O17 was synthesized under high‐pressure/high‐temperature conditions of 8 GPa and 1573 K in a multianvil apparatus. Single‐crystal X‐ray diffraction revealed a unique crystal structure that crystallizes in the orthorhombic non‐centrosymmetric space group Pmc21 (no. 26) with a=769.15(2), b=711.14(2), c=822.14(2) pm, V=0.450(1) nm3 and two formula units (Z=2) per unit cell...
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