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A route to salts of the [ClOF2]+ cation is described that does not require the parent fluoride ClOF3 as a starting material. These can be obtained when either metals such as Cr, Rh, Pd and Au, halides such as PtCl2, SnF2 and PbF4, or oxides such as B2O3, OsO4, GeO2, SnO and Sb2O4 are reacted with ClF3 and additional O2, where necessary, under UV irradiation. Cr, Rh, Pd, PtCl2, GeO2, and SnO formed...
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