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An anionic multifunctional porous metal organic framework (MOF), [Cu2THBA(H2O)2]·(C3H7NO)12·(H2O)10 (1) (H4THBA = p‐terphenyl‐3,2′′,3′′,5,5′′,5′′′‐ hexcarboxylic acid) with NbO‐type topology was synthesized and characterized. Due to multiple functional sites and suitable pore size, the desolvated compound 1a exhibits high separation selectivity for C2H2/CO2 of 30 and C2H2/CH4 of 131 at 1 kPa at room...
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