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An improved synthesis using microwave heating affords (C6H4PO(OCH3)2)2 in excellent isolated yield (95 %). The ligand properties of this bisphosphonateester were explored towards hard metal centers M2+ (M = Ca, UO2) and M3+ (M = La, Ce, Sm, Eu) resulting in coordination polymers, for which the reduction of ionic size of the central metal atom resulted in lower‐dimensional structural motifs as opposed...
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