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This review addresses the coordination chemistry (mainly) enabled by using the univalent [M(fluoroarene)2–3]+[Al(ORF)4]−‐salts (M=Ga, In; RF=C(CF3)3) as robust starting materials. In the course of this work, it became clear that the orbital energy of the ns2 (n=4, 5) lone pair in such [:M(L)n]+ cations reacts drastically depending on the quality of the ligand employed. Activation of the lone pair...
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