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A synthetic approach to synthesize the cationic trinuclear cluster with [Co3(μ3‐O)(μ‐OH)] core has been reported. A comparative study with the closely relevant polynuclear cluster containing [Co4(μ3‐O)4] active core has also been carried out along with a plausible pathway for these two clusters. The minor spectroscopic and electrochemical changes observed for the cores are quite significant to distinguish...
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