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The heterocubane‐like molecules [tBu2PhSiESn]4 (E = P (2), As (3)) and [(Me3Si)3SiPM]4 (M = Sn (4), Pb (5)) were obtained by the reaction of primary silyl phosphines or ‐arsines with M{N(SiMe3)2}2. Likewise, the reactions of the miscellaneously substituted arsine (Me3Si)3SiAs(SiMe3)2 (1) with MCl2 yielded the heterocubane species [(Me3Si)3SiAsM]4 (M = Sn (8), Pb (9)). The unique cage compounds [(t...
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