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The combination of hyperpolarized Xe with chemical exchange saturation transfer (Hyper‐CEST) is a powerful NMR technique to detect highly dilute concentrations of Xe binding sites using RF saturation pulses. Crucially, that combination of saturation pulse strength and duration that generates the maximal Hyper‐CEST effect is a priori unknown. In contrast to CEST in proton MRI, where the system reaches...
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