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Star polymers with a polyhedral oligomeric silsesquioxanes (POSS) core and eight partly fluorinated arms have been synthesized by reversible addition–fragmentation chain transfer polymerization. A macroCTA having eight chain transfer agent (CTA) molecules attached to a POSS core is prepared and used for the synthesis of star polymers by the R‐group approach. The arms are composed of statistical copolymers...
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