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The morphology and thermal stability of bead‐free and uniform electrospun pure polystyrene (PS) and PS/Ni nanocomposite fibers are investigated by SEM and TGA/DSC. A higher thermal stability is observed after introducing the nanoparticles in the polymer fibers. FT‐IR analysis indicates a physical entanglement rather than chemical bonding between the nanoparticles and the polystyrene matrix. The nanoparticles...
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