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Poly[1‐phenyl‐2‐(p‐trimethylsilyl)phenylacetylene] (PTMSDPA) with microporous and intramolecular stack structures in the bulk solid state can be used as a fluorescent water sensor for on‐line real‐time monitoring. A solubility parameter (δ) of PTMSDPA is estimated from the degree of swelling and solvation of the polymer in various organic solvents. When the PTMSDPA film is immersed in organic solvents...
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