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A nanoscale biodegradable polymersome with pH‐tuning on‐off membrane is prepared via the self‐assembly of poly(β‐amino ester)‐based amphiphilic copolymers. The pH‐sensitive polymersome‐like vesicle structure includes two layers that can encapsulate either hydrophobic or hydrophilic therapeutic drugs at physiological pH 7.4. Below a pH of 7.0, the polymersome membrane forms tunnels through which the...
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