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When alkynes were treated with diphenyl diselenide under an atmosphere of nitric oxide and oxygen, nitroselenation of the carbon‐carbon triple bond proceeded with a high regioselectivity to give the corresponding 1‐nitro‐2‐phenylseleno alkenes. Similarly, the nitroselenation of alkynes proceeded by the reaction of the alkynes with nitrogen dioxide. The stirring of the 1,2‐bis(phenylseleno) alkenes...
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