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It has been demonstrated that a variety of α‐phosphonovinyl arylsulfonates with electron‐neutral, ‐donating, and ‐withdrawing groups on the phenyl ring could be conveniently and efficiently prepared. In the presence of a Pd(OAc)2/SPhos‐based catalyst, various organoboron compounds could be employed as the nucleophilic coupling partners, such as organoboronic acids, boronate esters, and organotrifluoroborates...
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