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Attrition‐enhanced deracemization of two axially chiral nicotinamides, crystallizing as a conglomerate of a P21 crystal system, was performed. N,N‐Dialkylnicotinamides with substituents on the 2‐ and 4‐positions of the pyridine ring exhibited stable axial chirality due to rotationally restricted scaffolds for the Ar–C(=O)N bond. Crystallization of the racemic mixtures from the melt or attrition‐enhanced...
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