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Alkylidene acetoacetamides are useful building blocks for the preparation of a number of biologically active derivatives, including dehydro‐β‐amino‐acid‐containing peptidomimetics. A one‐pot two‐step protocol for the preparation of amino‐acid‐derived unsaturated acetoacetamides has been optimized. The use of microwave activation avoids, or at least decreases, the need for catalysts in both steps....
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