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An improved and convenient preparation of protected (S)‐isoserinal on a large scale is reported. This key intermediate was reacted through organocatalyzed aldol reaction or Wittig based chain extension and functionalization to give enantiopure 1,5,6‐trideoxy‐1,5‐imino‐hexitols such as 10a (L‐manno) and 10b (D‐gluco). These two compounds are of interest as glycosidase inhibitors. The elaborated organocatalytic...
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