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The catalytic hydrocarboxylation of styrenes derivatives and α,β‐unsaturated carbonyl compounds with CO2 (101.3 kPa) in the presence of an air‐stable rhodium catalyst was explored. The combination of [RhCl(cod)]2 (cod = cyclooctadiene) as a catalyst and diethylzinc as a hydride source allowed for effective hydrocarboxylation and provided the corresponding α‐aryl carboxylic acids in moderate to excellent...
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