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The osmium‐catalyzed oxyamination of chiral acyclic allylic alcohol derivatives bearing mono‐ and 1,1‐di‐substituted double bonds with benzyl N‐(4‐tosyloxy)carbamate proceeds with high regioselectivity and moderate levels of diastereoselectivity favoring the anti product. The observed stereoselectivity shows a clear and systematic trend with anti:syn ratios increasing in line with the size of substituent...
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