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We studied the spontaneous formation of chiral crystals of four diaryl ethers, 3‐phenoxybenzaldehyde, 1; 1,3‐dimethyl‐2‐phenoxybenzene, 2; di(4‐aminophenyl) ether, 3; and di(p‐tolyl) ether, 4. Compounds 1, 3, and 4 form conformationally chiral molecules in the solid state, while the chirality of 2 arises from the formation of supramolecular helices. Compound 1 is a liquid at ambient temperature, but...
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