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The H8BINOL‐based perfluoroalkyl ketone (S)‐2 is found to exhibit highly enantioselective fluorescent enhancements toward both unfunctionalized and functionalized chiral amines. It greatly expands the substrate scope of the corresponding BINOL‐based sensor. A dramatic solvent effect was observed for the reaction of the amines with compound (S)‐2. In DMF, cleavage of the perfluoroalkyl group of compound...
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