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High‐temperature chlorination of pristine C98 fullerene isomers separated by HPLC from the fullerene soot afforded crystals of C98Cl22 and C98Cl20. An X‐ray structure elucidation revealed, respectively, the presence of carbon cages of the most stable C2‐C98(248) and rather unstable C1‐C98(116), which represent the first isolated pentagon rule (IPR) isomers of fullerene C98 confirmed experimentally...
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