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Proton‐coupled electron transfer (PCET) was investigated in three covalent donor–bridge–acceptor molecules with different bridge lengths. Upon photoexcitation of their Ru(bpy)32+ (bpy=2,2′‐bipyridine) photosensitizer in acetonitrile, intramolecular long‐range electron transfer from a phenolic unit to Ru(bpy)32+ occurs in concert with release of the phenolic proton to pyrrolidine base. The kinetics...
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