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A new series of triphenylamine‐based ligands with one (TPA1PY), two (TPA2PY) or three pendant aza‐macrocycle(s) (TPA3PY) has been synthesised and studied by means of pH‐metric titrations, UV/Vis spectroscopy and fluorescence experiments. The affinity of these ligands for G‐quadruplex (G4) DNA and the selectivity they show for G4s over duplex DNA were investigated by Förster resonance energy transfer...
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